Platelet apparatus

Assessment of wear susceptibility

The platelet apparatus makes it possible to evaluate the wear behaviour of plastic compounds in melt processing or to determine the resistance of tool steels to given compounds.

2) Platelet apparatus mounted on single-screw extruder in operation.
3) Typical platelet surfaces after the extrusion test
3) Confocal chromatic microscopic image of a massively corrosively damaged platelet surface.

For this purpose, two equal-sized cuboid pieces (15 x 12 x 5 mm) of the test material are mounted opposite each other in a frame in such a way that a gap of 10 mm width, 12 mm length and a height of 0.2-1 mm is created through the two plates (Fig. 1). The frame is mounted in a measuring tool, which is flanged to a single-screw extruder.

The melt is extruded through the gap formed by the platelets (Fig. 2). The shear flow in the slot, together with the abrasive and corrosive properties of the melt, causes material to be removed from the platelets. The wear is quantified based the weight loss of the platelets

Abrasive melts primarily result in uniform material removal. Corrosive melts usually cause an irregular surface structure. This can be visualised very well using confocal chromatic measurement technology (Fig. 3). For a more detailed metallographic analysis of the wear pattern, SEM/EDX electron microscopy can be used.

To assess the corrosiveness of compounds or to establish a ranking within an ensemble of compounds, we use tool steel 1.2329 (hardened) as standard. This is widely used in plastics processing and can be found in non-return valves, screws and injection moulds. Other steels are also used in consultation with our customers, depending on the specific nature of the compounds to be assessed.

In the comparative evaluation of materials, which may also involve corresponding coatings, our customer specifies the relevant compounds. We can also suggest suitable ones.

The interaction between the plastic melt and the material in the platelet apparatus comes very close to the real situation in plastics processing machines. The suitability of this test method has therefore been demonstrated in numerous bilateral projects with industry as well as in publicly funded projects, both in the development of formulations and in the selection of materials for the housings or screws of plastics processing machines.

We offer:

  • Quantification of the corrosiveness and abrasion behaviour of plastics towards to a tool steel. Typically, 25 kg of the respective material is required.
  • Testing tool steels or coatings on steels for corrosion and/or abrasion resistance. As a rule, 25-50 kg of a plastic grade is used to evaluate a steel grade.
  • Investigation of wear mechanisms (SEM/EDX studies).
  • Based on LBF's expertise in formulation and additive research: development of formulations aimed at minimising corrosiveness, e.g. flame-retardant polymers.
  • Support during the development phase and transfer to industrial processing.

Publications:

  • www.compoundingworld.com, April 2018, "Targeting a hot market", p. 19-21.
  • Le Gal, A.; Ziemer, W. and Kern, W.: Zündeln unerwünscht: Halogenfreie und verschleißarme Hochtemperatur-Compounds auf Polyamidbasis. Kunststoffe 2016, 2, 74-76.
  • Steinhoff, B. in Final report of the joint research project (BMBF) " Kratzfeste Polymere durch ein neues Verfahren zur Herstellung von Nanocompounds - NaNo-Scratch ", K. Lehmann (EVONIK) (Ed.) 2011.
  • Rudschuck, M.: Verschleißreduzierung bei der Verarbeitung nanoskaliger Füllstoffe, DKI annual report ISBN 1618-0062; 6 (2005) 116-119.
  • Rudschuck, M.; Iarskaia, E. and Hartig, H.: Wear protection in plastics processing by ceramic compounds, Materialwissenschaft und Werkstofftechnik 37, 4 (2006) 329-332.